Ni(II) – ONO ve ONNO Tipi Schiff Bazı Komplekslerinin Termal Bozunmalarını Kullanarak NiO Nanopartiküllerinin Sentezi ve Karakterizasyonu

Five different Nickel (II) complexes were prepared using a ONNO type Schiff base bis-N;N’(salicylidene)-1,3-propanediamine (LH2) and an ONO N(2-hydroxy)salicylaldimine (SAPH2) in the presence of NH3 or amine NiO nanoparticles obtained with thermal decomposition this air. The bases have been characterized by element analysis, IR spectroscopy, Thermogravimetry (TG), 1HNMR 13CNMR Mass Spectrometry (MS), Atomic absorption spectrometry (AAS), Scanning Electron Microscopy (SEM). surface area nanoparticle material was measured Brunauer-Emmett-Teller (BET) method. products investigated XRD, SEM technics. investigations showed that due to very little solubility two consequently they precipitated form nanoparticles. In addition, it observed insoluble are converted result decomposition.